Information card for entry 1557608

Structure parameters

• Formula: C22 H48 Cl2 N2 Ni O3 P2 U
• Calculated formula: C22 H48 Cl2 N2 Ni O3 P2 U
• Title of publication: Construction of heterometallic clusters with multiple uranium‒metal bonds by using dianionic nitrogen‒phosphorus ligands
• Authors of publication: Feng, Genfeng; McCabe, Karl N.; Wang, Shuao; Maron, Laurent; Zhu, Congqing
• Journal of publication: Chemical Science
• Year of publication: 2020
• Journal volume: 11
• Journal issue: 29
• Pages of publication: 7585 - 7592
• a: 11.3508 ± 0.0018 Å
• b: 12.914 ± 0.002 Å
• c: 20.597 ± 0.004 Å
• α: 90°
• β: 95.165 ± 0.007°
• γ: 90°
• Cell volume: 3006.9 ± 0.9 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1126
• Residual factor for significantly intense reflections: 0.0977
• Weighted residual factors for significantly intense reflections: 0.2146
• Weighted residual factors for all reflections included in the refinement: 0.2235
• Goodness-of-fit parameter for all reflections included in the refinement: 1.112
• Diffraction radiation wavelength: 1.34139 Å
• Diffraction radiation type: GaKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No