Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 1557872
Preview
Coordinates | 1557872.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C32 H33 F6 N O4 |
---|---|
Calculated formula | C32 H33 F6 N O4 |
Title of publication | Synthesis and properties of hypervalent electron-rich pentacoordinate nitrogen compounds |
Authors of publication | Yan, Chenting; Takeshita, Masato; Nakatsuji, Jun-ya; Kurosaki, Akihiro; Sato, Kaoko; Shang, Rong; Nakamoto, Masaaki; Yamamoto, Yohsuke; Adachi, Yohei; Furukawa, Ko; Kishi, Ryohei; Nakano, Masayoshi |
Journal of publication | Chemical Science |
Year of publication | 2020 |
Journal volume | 11 |
Journal issue | 19 |
Pages of publication | 5082 - 5088 |
a | 10.089 ± 0.0004 Å |
b | 11.8293 ± 0.0005 Å |
c | 13.7884 ± 0.0006 Å |
α | 97.567 ± 0.001° |
β | 107.754 ± 0.001° |
γ | 95.274 ± 0.001° |
Cell volume | 1538.29 ± 0.11 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.046 |
Residual factor for significantly intense reflections | 0.0406 |
Weighted residual factors for significantly intense reflections | 0.1065 |
Weighted residual factors for all reflections included in the refinement | 0.1114 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.039 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/1557872.html
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.