Information card for entry 1558929

Structure parameters

• Formula: C51 H43 B F24 N Ni O P
• Calculated formula: C51 H43 B F24 N Ni O P
• Title of publication: A N-bridged strategy enables hemilabile phosphine‒carbonyl palladium and nickel catalysts to mediate ethylene polymerization and copolymerization with polar vinyl monomers
• Authors of publication: Cui, Lei; Jian, Zhongbao
• Journal of publication: Polymer Chemistry
• Year of publication: 2020
• Journal volume: 11
• Journal issue: 38
• Pages of publication: 6187 - 6193
• a: 12.6795 ± 0.0003 Å
• b: 19.6724 ± 0.0004 Å
• c: 21.4947 ± 0.0004 Å
• α: 90°
• β: 97.371 ± 0.001°
• γ: 90°
• Cell volume: 5317.25 ± 0.19 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0632
• Residual factor for significantly intense reflections: 0.0553
• Weighted residual factors for significantly intense reflections: 0.1392
• Weighted residual factors for all reflections included in the refinement: 0.1475
• Goodness-of-fit parameter for all reflections included in the refinement: 1.003
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No