Information card for entry 1558954

Structure parameters

• Common name: 3,3-Dimethyl-1,5,9-trioxacyclododecane Lithium Perchlorate
• Formula: C11 H22 Cl Li O7
• Calculated formula: C11 Cl Li O7
• Title of publication: 12-Crown-3 Type Li+ Complexes: Structures of 3,3-Dimethyl-1,5,9-trioxacyclododecane Lithium Perchlorate and 3-Methoxymethyl-3-methyl-1,5,9-trioxacyclododecane Lithium Perchlorate Hemihydrate
• Authors of publication: Tinant, Bernard; Declercq, Jean-Paul; Fredriksen, Siw B.; Dale, Johannes
• Journal of publication: Acta Chemica Scandinavica
• Year of publication: 1993
• Journal volume: 47
• Pages of publication: 663 - 667
• a: 16.905 ± 0.002 Å
• b: 10.157 ± 0.001 Å
• c: 9.097 ± 0.001 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1562 ± 0.3 ų
• Ambient diffraction temperature: 293 K
• Number of distinct elements: 5
• Space group number: 33
• Hermann-Mauguin space group symbol: P n a 21
• Hall space group symbol: P 2c -2n
• Residual factor for significantly intense reflections: 0.08
• Weighted residual factors for significantly intense reflections: 0.088
• Goodness-of-fit parameter for all reflections included in the refinement: 0.58
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No