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Information card for entry 1559036
Preview
Coordinates | 1559036.cif |
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Original paper (by DOI) | HTML |
Common name | [C29 H32 N4 Rh]+ [P F6]- [CH2 Cl2] (H2 O) |
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Formula | C30 H34.5 Cl2 F6 N4 O0.25 P Rh |
Calculated formula | C30 Cl2 F6 N4 O0.25 P Rh |
Title of publication | Two Analogous Azamacrocyclic Compounds of Cobalt(III) and Rhodium(III) Containing Pendent Metal‒Carbon Bonds. Synthesis and Comparison by NMR and X-Ray Structure Determinations |
Authors of publication | Kofod, Pauli; Alcock, Nathaniel W.; Moore, Peter |
Journal of publication | Acta Chemica Scandinavica |
Year of publication | 1993 |
Journal volume | 47 |
Pages of publication | 1083 - 1090 |
a | 10.197 ± 0.005 Å |
b | 11.36 ± 0.005 Å |
c | 14.046 ± 0.006 Å |
α | 81.95 ± 0.03° |
β | 70.84 ± 0.04° |
γ | 77.69 ± 0.04° |
Cell volume | 1497.3 ± 1.2 Å3 |
Ambient diffraction temperature | 290 K |
Number of distinct elements | 8 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.083 |
Residual factor for significantly intense reflections | 0.065 |
Weighted residual factors for significantly intense reflections | 0.083 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.47 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71069 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/1559036.html
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