Information card for entry 1559078

Structure parameters

• Common name: [CoL(NCCH3)2Cl]CoCl4 (L = 1,4,7-Trimethyl-1,4,7-triazacyclononane)
• Formula: C13 H27 Cl5 Co2 N5
• Calculated formula: C11.5 Cl6.5 Co2 N5
• Title of publication: The Structure of a Novel Complex of Cobalt(III) with a Tridentate Macrocyclic Ligand with Tertiary Amine Donors, [CoL(NCCH3)2Cl]CoCl4 (L = 1,4,7-Trimethyl-1,4,7-triazacyclononane)
• Authors of publication: Searle, Graeme H.; Wang, Dong-Ni; Larsen, Sine; Larsen, Erik
• Journal of publication: Acta Chemica Scandinavica
• Year of publication: 1992
• Journal volume: 46
• Pages of publication: 38 - 42
• a: 12.172 ± 0.003 Å
• b: 14.331 ± 0.004 Å
• c: 26.032 ± 0.005 Å
• α: 90°
• β: 98.37 ± 0.02°
• γ: 90°
• Cell volume: 4492.6 ± 1.9 ų
• Ambient diffraction temperature: 110 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for significantly intense reflections: 0.058
• Weighted residual factors for significantly intense reflections: 0.062
• Goodness-of-fit parameter for all reflections included in the refinement: 1.1
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No