Information card for entry 1561155

Structure parameters

• Formula: Ca0.69 Nd0.31 O5 Si V
• Calculated formula: Ca0.6849 Nd0.3151 O5 Si V
• Title of publication: Facile in-situ reduction: Crystal growth and magnetic studies of reduced vanadium (III/IV) silicates CaxLn1−xVSiO5 (Ln = Ce‒Nd, Sm‒Lu, Y)
• Authors of publication: Abeysinghe, Dileka; Smith, Mark D.; Morrison, Gregory; Yeon, Jeongho; zur Loye, Hans-Conrad
• Journal of publication: Journal of Solid State Chemistry
• Year of publication: 2018
• Journal volume: 260
• Pages of publication: 80 - 86
• a: 6.5633 ± 0.0004 Å
• b: 8.7999 ± 0.0005 Å
• c: 6.9335 ± 0.0004 Å
• α: 90°
• β: 112.803 ± 0.0016°
• γ: 90°
• Cell volume: 369.16 ± 0.04 ų
• Cell temperature: 297 ± 2 K
• Ambient diffraction temperature: 297 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0211
• Residual factor for significantly intense reflections: 0.0196
• Weighted residual factors for significantly intense reflections: 0.0537
• Weighted residual factors for all reflections included in the refinement: 0.0543
• Goodness-of-fit parameter for all reflections included in the refinement: 1.143
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No