Information card for entry 1561190

Structure parameters

• Formula: C72 H162 K2 N4 O24 Si6 U2
• Calculated formula: C72 H162 K2 N4 O24 Si6 U2
• Title of publication: Single metal four-electron reduction by U(ii) and masked "U(ii)" compounds.
• Authors of publication: Modder, Dieuwertje K.; Palumbo, Chad T.; Douair, Iskander; Scopelliti, Rosario; Maron, Laurent; Mazzanti, Marinella
• Journal of publication: Chemical science
• Year of publication: 2021
• Journal volume: 12
• Journal issue: 17
• Pages of publication: 6153 - 6158
• a: 14.382 ± 0.002 Å
• b: 17.661 ± 0.003 Å
• c: 21.819 ± 0.004 Å
• α: 90°
• β: 92.012 ± 0.009°
• γ: 90°
• Cell volume: 5538.6 ± 1.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100.15 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.117
• Residual factor for significantly intense reflections: 0.0592
• Weighted residual factors for significantly intense reflections: 0.1241
• Weighted residual factors for all reflections included in the refinement: 0.1665
• Goodness-of-fit parameter for all reflections included in the refinement: 1.135
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No