Information card for entry 1561347

Structure parameters

• Formula: C40 H106 Co4 N8 O133 Si2 W24
• Calculated formula: C40 H106 Co4 N8 O133 Si2 W24
• Title of publication: Two supramolecular complexes based on polyoxometalates and Co-EDTA units via covalent connection or non-covalent interaction
• Authors of publication: Teng, Chunlin; Xiao, Hanxi; Cai, Qing; Tang, Jianting; Cai, Tiejun; Deng, Qian
• Journal of publication: Journal of Solid State Chemistry
• Year of publication: 2016
• Journal volume: 243
• Pages of publication: 146 - 153
• a: 13.0101 ± 0.0005 Å
• b: 14.5594 ± 0.0006 Å
• c: 19.4444 ± 0.0008 Å
• α: 81.734 ± 0.003°
• β: 75.23 ± 0.004°
• γ: 85.989 ± 0.003°
• Cell volume: 3522.3 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0954
• Residual factor for significantly intense reflections: 0.0682
• Weighted residual factors for significantly intense reflections: 0.1804
• Weighted residual factors for all reflections included in the refinement: 0.1985
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation wavelength: 0.71 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No