Information card for entry 1561465

Structure parameters

• Formula: F Ge4 Na5 Nd4 O16
• Calculated formula: F Ge4 Na5 Nd4 O16
• Title of publication: A5RE4X[TO4]4 crystal growth: Fluoride flux synthesis of Na5Ln4F[GeO4]4 (Ln=Pr, Nd), the first quaternary germanate oxyfluorides
• Authors of publication: Latshaw, Allison M.; Wilkins, Branford O.; Morrison, Gregory; Smith, Mark D.; zur Loye, Hans-Conrad
• Journal of publication: Journal of Solid State Chemistry
• Year of publication: 2016
• Journal volume: 239
• Pages of publication: 200 - 203
• a: 12.0642 ± 0.0017 Å
• b: 12.0642 ± 0.0017 Å
• c: 5.6674 ± 0.0011 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 824.9 ± 0.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 82
• Hermann-Mauguin space group symbol: I -4
• Hall space group symbol: I -4
• Residual factor for all reflections: 0.0212
• Residual factor for significantly intense reflections: 0.0209
• Weighted residual factors for significantly intense reflections: 0.0559
• Weighted residual factors for all reflections included in the refinement: 0.0561
• Goodness-of-fit parameter for all reflections included in the refinement: 1.105
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No