Information card for entry 1561548

Structure parameters

• Formula: C47 H91 B Ge9 K N3 Si8
• Calculated formula: C47 H91 B Ge9 K N3 Si8
• Title of publication: FLP-type Nitrile Activation and Cyclic Ether Ring Opening by Halo-Borane Nonagermanide-Cluster Lewis Acid-Base-Pairs
• Authors of publication: Wallach, Chistoph; Geitner, Felix; Fässler, Thomas F
• Journal of publication: Chemical Science
• Year of publication: 2021
• a: 13.7573 ± 0.0004 Å
• b: 9.2613 ± 0.0003 Å
• c: 28.4239 ± 0.001 Å
• α: 90 ± 0.003°
• β: 94.438 ± 0.003°
• γ: 90 ± 0.002°
• Cell volume: 3610.6 ± 0.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0296
• Residual factor for significantly intense reflections: 0.0253
• Weighted residual factors for significantly intense reflections: 0.0556
• Weighted residual factors for all reflections included in the refinement: 0.0574
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No