Information card for entry 1561659

Structure parameters

• Formula: C10 H14 N14 O9 Pb4
• Calculated formula: C10 H14 N14 O9 Pb4
• Title of publication: A novel tetranuclear Pb2+ compound based on ethylenediaminetetraacetate and azide mixed-ligands: Synthesis, structure and properties
• Authors of publication: Liu, Dong-Sheng; Qiu, Zhi-Jun; Xiao, Yang-Lan; Shen, Yu-Jun; Zhou, Qi; Chen, Wen-Tong; Sui, Yan
• Journal of publication: Journal of Solid State Chemistry
• Year of publication: 2019
• Journal volume: 279
• Pages of publication: 120952
• a: 13.541 ± 0.0004 Å
• b: 8.8827 ± 0.0003 Å
• c: 19.1758 ± 0.0005 Å
• α: 90°
• β: 94.049 ± 0.002°
• γ: 90°
• Cell volume: 2300.72 ± 0.12 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0442
• Residual factor for significantly intense reflections: 0.0348
• Weighted residual factors for significantly intense reflections: 0.0799
• Weighted residual factors for all reflections included in the refinement: 0.0844
• Goodness-of-fit parameter for all reflections included in the refinement: 1.056
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No