Information card for entry 1562228

Structure parameters

• Formula: C36 H45 Au Cl F6 N P Sb
• Calculated formula: C36 H45 Au Cl F6 N P Sb
• Title of publication: Oxidative additions of alkynyl/vinyl iodides to gold and gold-catalyzed vinylation reactions triggered by the MeDalphos Ligand
• Authors of publication: Rodriguez, Jessica; Tabey, Alexis; Ladeira, Sonia; Bourissou, Didier
• Journal of publication: Chemical Science
• Year of publication: 2021
• a: 29.91 ± 0.004 Å
• b: 9.8604 ± 0.0014 Å
• c: 28.71 ± 0.004 Å
• α: 90°
• β: 119.225 ± 0.004°
• γ: 90°
• Cell volume: 7389.5 ± 1.8 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 8
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0657
• Residual factor for significantly intense reflections: 0.0573
• Weighted residual factors for significantly intense reflections: 0.1355
• Weighted residual factors for all reflections included in the refinement: 0.1384
• Goodness-of-fit parameter for all reflections included in the refinement: 1.257
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No