Information card for entry 1562230

Structure parameters

• Formula: C33 H47 Au Cl F6 N O2 P Sb
• Calculated formula: C33 H47 Au Cl F6 N O2 P Sb
• Title of publication: Oxidative additions of alkynyl/vinyl iodides to gold and gold-catalyzed vinylation reactions triggered by the MeDalphos Ligand
• Authors of publication: Rodriguez, Jessica; Tabey, Alexis; Ladeira, Sonia; Bourissou, Didier
• Journal of publication: Chemical Science
• Year of publication: 2021
• a: 9.7524 ± 0.0011 Å
• b: 25.856 ± 0.003 Å
• c: 14.5514 ± 0.0017 Å
• α: 90°
• β: 106.77 ± 0.003°
• γ: 90°
• Cell volume: 3513.2 ± 0.7 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 9
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0796
• Residual factor for significantly intense reflections: 0.0395
• Weighted residual factors for significantly intense reflections: 0.0686
• Weighted residual factors for all reflections included in the refinement: 0.0805
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No