Information card for entry 1562274

Structure parameters

• Formula: C32 H40 N8 Ni O16
• Calculated formula: C32 H40 N8 Ni O16
• Title of publication: Syntheses, crystal structures, and characterization of three 1D, 2D and 3D complexes based on mixed multidentate N- and O-donor ligands
• Authors of publication: Yang, Huai-Xia; Liang, Zhen; Hao, Bao-Lian; Meng, Xiang-Ru
• Journal of publication: Journal of Solid State Chemistry
• Year of publication: 2014
• Journal volume: 218
• Pages of publication: 23 - 31
• a: 7.3391 ± 0.0015 Å
• b: 9.4757 ± 0.0019 Å
• c: 13.417 ± 0.003 Å
• α: 85.59 ± 0.03°
• β: 76.21 ± 0.03°
• γ: 85.08 ± 0.03°
• Cell volume: 901.3 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0634
• Residual factor for significantly intense reflections: 0.0607
• Weighted residual factors for significantly intense reflections: 0.1509
• Weighted residual factors for all reflections included in the refinement: 0.1535
• Goodness-of-fit parameter for all reflections included in the refinement: 1.052
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No