Crystallography Open Database

Information card for entry 1562657

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Coordinates	1562657.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C16 H72 B22 N10 O58 V6
Calculated formula	C16 H64 B22 N10 O58 V6
Title of publication	Hydrothermal syntheses, crystal structures and characterization of new vanadoborates: The novel decorated cage cluster [V6B22O44(OH)10]
Authors of publication	Liu, Xing; Zhou, Jian; An, Litao; Chen, Rong; Hu, Feilong; Tang, Qiuling
Journal of publication	Journal of Solid State Chemistry
Year of publication	2013
Journal volume	201
Pages of publication	79 - 84
a	23.943 ± 0.005 Å
b	12.552 ± 0.002 Å
c	23.198 ± 0.005 Å
α	90°
β	118.511 ± 0.005°
γ	90°
Cell volume	6126 ± 2 Å³
Cell temperature	223 ± 2 K
Ambient diffraction temperature	223 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0908
Residual factor for significantly intense reflections	0.0805
Weighted residual factors for significantly intense reflections	0.1977
Weighted residual factors for all reflections included in the refinement	0.2066
Goodness-of-fit parameter for all reflections included in the refinement	1.03
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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