Information card for entry 1562773

Structure parameters

• Formula: C30 H41 B Cu2 N6 O48 W12
• Calculated formula: C30 H24 B Cu2 N6 O48 W12
• Title of publication: An unusual 3D interdigitated architecture assembled from Keggin polyoxometalates and dinuclear copper(II) complexes
• Authors of publication: Pang, Haijun; Yang, Ming; Kang, Lu; Ma, Huiyuan; Liu, Bo; Li, Shaobin; Liu, Heng
• Journal of publication: Journal of Solid State Chemistry
• Year of publication: 2013
• Journal volume: 198
• Pages of publication: 440 - 444
• a: 13.116 ± 0.005 Å
• b: 15.76 ± 0.005 Å
• c: 14.792 ± 0.005 Å
• α: 90 ± 0.005°
• β: 94.418 ± 0.005°
• γ: 90 ± 0.005°
• Cell volume: 3048.5 ± 1.8 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 7
• Hermann-Mauguin space group symbol: P 1 n 1
• Hall space group symbol: P -2yac
• Residual factor for all reflections: 0.0546
• Residual factor for significantly intense reflections: 0.0432
• Weighted residual factors for significantly intense reflections: 0.0865
• Weighted residual factors for all reflections included in the refinement: 0.0925
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No