Information card for entry 1563300

Structure parameters

• Formula: C60 H70 As2 N10 Ni4 O73 W18
• Calculated formula: C60 H64 As2 N10 Ni4 O73 W18
• Title of publication: Assemblies based on the directing effect of non-classical W18 anionic clusters and the rod-like trans-1,2-di-(4-pyridyl)-ethylen (bpe)
• Authors of publication: Han, Zhangang; Wang, Yanna; Song, Xuejun; Huang, Jiao; Zhai, Xueliang
• Journal of publication: Journal of Solid State Chemistry
• Year of publication: 2011
• Journal volume: 184
• Journal issue: 3
• Pages of publication: 690 - 697
• a: 15.5969 ± 0.001 Å
• b: 17.8244 ± 0.0011 Å
• c: 20.5325 ± 0.0013 Å
• α: 67.74 ± 0.001°
• β: 89.915 ± 0.001°
• γ: 85.917 ± 0.001°
• Cell volume: 5267.3 ± 0.6 ų
• Cell temperature: 273 ± 2 K
• Ambient diffraction temperature: 273 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0926
• Residual factor for significantly intense reflections: 0.0627
• Weighted residual factors for significantly intense reflections: 0.1705
• Weighted residual factors for all reflections included in the refinement: 0.2051
• Goodness-of-fit parameter for all reflections included in the refinement: 1.003
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No