Information card for entry 1563353

Structure parameters

• Formula: C4 H6 Ge2 K8 Na2 O108 W22 Yb2
• Calculated formula: C4 H6 Ge2 K8 Na2 O108 W22 Yb2
• Title of publication: A new series of lanthanoid containing Keggin-type germanotungstates with acetate chelators: [{Ln(CH3COO)GeW11O39(H2O)}2]12− {Ln=EuIII, GdIII, TbIII, DyIII, HoIII, ErIII, TmIII, and YbIII}
• Authors of publication: Hussain, Firasat; Sandriesser, Stefan; Speldrich, Manfred; Patzke, Greta R.
• Journal of publication: Journal of Solid State Chemistry
• Year of publication: 2011
• Journal volume: 184
• Journal issue: 1
• Pages of publication: 214 - 219
• a: 19.9221 ± 0.0002 Å
• b: 12.5672 ± 0.0001 Å
• c: 20.9741 ± 0.0002 Å
• α: 90°
• β: 111.263 ± 0.001°
• γ: 90°
• Cell volume: 4893.71 ± 0.08 ų
• Cell temperature: 183 ± 2 K
• Ambient diffraction temperature: 183 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.061
• Residual factor for significantly intense reflections: 0.0453
• Weighted residual factors for significantly intense reflections: 0.1271
• Weighted residual factors for all reflections included in the refinement: 0.1316
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No