Information card for entry 1563585

Structure parameters

• Formula: C28 H48 N4 Nd4 O78 Si W12
• Calculated formula: C28 H32 N4 Nd4 O74 Si W12
• Title of publication: Syntheses, structures and properties of 3D inorganic‒organic hybrid frameworks constructed from lanthanide polymer and Keggin-type tungstosilicate
• Authors of publication: Gao, Yuanzhe; Xu, Yanqing; Han, Zhangang; Li, Chunhong; Cui, Fengyun; Chi, Yingnan; Hu, Changwen
• Journal of publication: Journal of Solid State Chemistry
• Year of publication: 2010
• Journal volume: 183
• Journal issue: 5
• Pages of publication: 1000 - 1006
• a: 21.917 ± 0.002 Å
• b: 21.917 ± 0.002 Å
• c: 16.5868 ± 0.0018 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 7967.6 ± 1.3 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 7
• Space group number: 88
• Hermann-Mauguin space group symbol: I 41/a :2
• Hall space group symbol: -I 4ad
• Residual factor for all reflections: 0.0971
• Residual factor for significantly intense reflections: 0.061
• Weighted residual factors for significantly intense reflections: 0.1257
• Weighted residual factors for all reflections included in the refinement: 0.1472
• Goodness-of-fit parameter for all reflections included in the refinement: 1.125
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No