Information card for entry 1563832

Structure parameters

• Formula: C89 H81 Cl3 Ge4 N4 O14
• Calculated formula: C89 H81 Cl3 Ge4 N4 O14
• Title of publication: (S)-N-[(2-hydroxynaphthalen-1-yl)methylidene]valine ‒ A valuable ligand for the preparation of chiral complexes
• Authors of publication: Schwarzer, Sandra; Böhme, Uwe; Fels, Sabine; Günther, Betty; Brendler, Erica
• Journal of publication: Inorganica Chimica Acta
• Year of publication: 2018
• Journal volume: 483
• Pages of publication: 136 - 147
• a: 11.4185 ± 0.0005 Å
• b: 12.0876 ± 0.0006 Å
• c: 16.5054 ± 0.0008 Å
• α: 110.74 ± 0.004°
• β: 100.151 ± 0.004°
• γ: 100.061 ± 0.004°
• Cell volume: 2026.38 ± 0.19 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0812
• Residual factor for significantly intense reflections: 0.0564
• Weighted residual factors for significantly intense reflections: 0.158
• Weighted residual factors for all reflections included in the refinement: 0.1726
• Goodness-of-fit parameter for all reflections included in the refinement: 0.961
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No