Information card for entry 1564891

Structure parameters

• Formula: C67 H58 B Cl2 F29 N P Pd
• Calculated formula: C67 H58 B Cl2 F29 N P Pd
• Title of publication: Highly efficient vinylic addition polymerization of 5-vinyl-2-norbornene using benzylic palladium complexes as precatalysts
• Authors of publication: Pérez-Ortega, Ignacio; Albéniz, Ana C.
• Journal of publication: Polymer Chemistry
• Year of publication: 2021
• Journal volume: 12
• Journal issue: 41
• Pages of publication: 5963 - 5969
• a: 13.4173 ± 0.0007 Å
• b: 15.6707 ± 0.0007 Å
• c: 18.5278 ± 0.0008 Å
• α: 84.761 ± 0.004°
• β: 70.245 ± 0.004°
• γ: 89.96 ± 0.004°
• Cell volume: 3649.1 ± 0.3 ų
• Cell temperature: 298 K
• Ambient diffraction temperature: 298 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.091
• Residual factor for significantly intense reflections: 0.0506
• Weighted residual factors for significantly intense reflections: 0.1067
• Weighted residual factors for all reflections included in the refinement: 0.1345
• Goodness-of-fit parameter for all reflections included in the refinement: 1.013
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No