Information card for entry 1565203

Structure parameters

• Formula: C40 H54 N8 O4 Rh2
• Calculated formula: C40 H54 N8 O4 Rh2
• Title of publication: Rhodium and iridium NNO-Scorpionate complexes: synthesis, structure, and reactivity with aluminum alkyls
• Authors of publication: Yokley, Timothy W.; Schley, Nathan D.; Brewster, Timothy P.
• Journal of publication: Inorganica Chimica Acta
• Year of publication: 2020
• Journal volume: 506
• Pages of publication: 119529
• a: 10.6115 ± 0.0003 Å
• b: 10.8579 ± 0.0003 Å
• c: 17.2908 ± 0.0007 Å
• α: 93.506 ± 0.002°
• β: 102.353 ± 0.003°
• γ: 92.412 ± 0.002°
• Cell volume: 1939.34 ± 0.11 ų
• Cell temperature: 99.94 ± 0.14 K
• Ambient diffraction temperature: 99.94 ± 0.14 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0746
• Residual factor for significantly intense reflections: 0.0512
• Weighted residual factors for significantly intense reflections: 0.0862
• Weighted residual factors for all reflections included in the refinement: 0.0935
• Goodness-of-fit parameter for all reflections included in the refinement: 1.058
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No