Information card for entry 1566423

Structure parameters

• Formula: C23 H29 N O5 S Si
• Calculated formula: C23 H29 N O5 S Si
• Title of publication: Intramolecular Photochemical [2+1]-Cycloadditions of Nucleophilic Siloxy Carbenes
• Authors of publication: Bunyamin, Amanda; Hua, Carol; Polyzos, Anastasios; Priebbenow, Daniel
• Journal of publication: Chemical Science
• Year of publication: 2022
• a: 8.92 ± 0.0018 Å
• b: 18.338 ± 0.004 Å
• c: 14.723 ± 0.003 Å
• α: 90°
• β: 99.61 ± 0.03°
• γ: 90°
• Cell volume: 2374.5 ± 0.9 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.05
• Residual factor for significantly intense reflections: 0.0465
• Weighted residual factors for significantly intense reflections: 0.1244
• Weighted residual factors for all reflections included in the refinement: 0.131
• Goodness-of-fit parameter for all reflections included in the refinement: 1.072
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: Synchrotron
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No