Crystallography Open Database

Information card for entry 1566524

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Coordinates	1566524.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C74 H104 Ga2 N8 Sb2
Calculated formula	C74 H104 Ga2 N8 Sb2
Title of publication	Synthesis of Distibiranes and Azadistibiranes by Cycloaddition Reactions of Distibenes with Diazomethanes and Azides
Authors of publication	Weinert, Hanns Micha; Wölper, Christoph; Schulz, Stephan
Journal of publication	Chemical Science
Year of publication	2022
a	10.4552 ± 0.0004 Å
b	11.9732 ± 0.0004 Å
c	14.9227 ± 0.0005 Å
α	93.2189 ± 0.0014°
β	97.3354 ± 0.0014°
γ	107.995 ± 0.0014°
Cell volume	1753.06 ± 0.11 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0219
Residual factor for significantly intense reflections	0.0191
Weighted residual factors for significantly intense reflections	0.0525
Weighted residual factors for all reflections included in the refinement	0.0543
Goodness-of-fit parameter for all reflections included in the refinement	1.079
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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