Information card for entry 1566533

Structure parameters

• Formula: C68 H110 Ga2 N8 Sb2 Si2
• Calculated formula: C66 H107 Ga2 N7 Sb2 Si2
• Title of publication: Synthesis of Distibiranes and Azadistibiranes by Cycloaddition Reactions of Distibenes with Diazomethanes and Azides
• Authors of publication: Weinert, Hanns Micha; Wölper, Christoph; Schulz, Stephan
• Journal of publication: Chemical Science
• Year of publication: 2022
• a: 11.889 ± 0.002 Å
• b: 18.46 ± 0.004 Å
• c: 33.366 ± 0.007 Å
• α: 90°
• β: 96.36 ± 0.011°
• γ: 90°
• Cell volume: 7278 ± 3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0615
• Residual factor for significantly intense reflections: 0.0404
• Weighted residual factors for significantly intense reflections: 0.0794
• Weighted residual factors for all reflections included in the refinement: 0.0866
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No