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Information card for entry 1567168
Preview
Coordinates | 1567168.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C28 H24 O4 |
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Calculated formula | C28 H24 O4 |
Title of publication | Cu(ii)/SPDO complex catalyzed asymmetric Baeyer-Villiger oxidation of 2-arylcyclobutanones and its application for the total synthesis of eupomatilones 5 and 6. |
Authors of publication | Zhang, Chang-Sheng; Shao, Ya-Ping; Zhang, Fu-Min; Han, Xue; Zhang, Xiao-Ming; Zhang, Kun; Tu, Yong-Qiang |
Journal of publication | Chemical science |
Year of publication | 2022 |
Journal volume | 13 |
Journal issue | 28 |
Pages of publication | 8429 - 8435 |
a | 8.6793 ± 0.0001 Å |
b | 22.7043 ± 0.0003 Å |
c | 11.0413 ± 0.0001 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 2175.77 ± 0.04 Å3 |
Cell temperature | 298.23 ± 0.1 K |
Ambient diffraction temperature | 298.23 ± 0.1 K |
Number of distinct elements | 3 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.0393 |
Residual factor for significantly intense reflections | 0.0368 |
Weighted residual factors for significantly intense reflections | 0.101 |
Weighted residual factors for all reflections included in the refinement | 0.1025 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.066 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/1567168.html
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