Information card for entry 1567182

Structure parameters

• Chemical name: Bis{[amino(iminiumyl)methyl]urea} tetrakis{2-[(dimethylamino)(iminiumyl)methyl]guanidine} di-μ~6~-oxido-tetra-μ~3~-oxido-tetradeca-μ~2~-oxido-octaoxidodecavanadium(V) tetrahydrate
• Formula: C20 H70 N28 O34 V10
• Calculated formula: C20 H70 N28 O34 V10
• Title of publication: Bis{[amino(iminiumyl)methyl]urea} tetrakis{2-[(dimethylamino)(iminiumyl)methyl]guanidine} di-μ~6~-oxido-tetra-μ~3~-oxido-tetradeca-μ~2~-oxido-octaoxidodecavanadium(V) tetrahydrate
• Authors of publication: Pérez-Benítez, Aarón; Ariza-Ramírez, Jorge Luis; Fortis-Valera, Monserrat; Arroyo-Carmona, Rosa Elena; Martínez de la Luz, María Isabel; Ramírez-Contreras, Diego; Bernès, Sylvain
• Journal of publication: IUCrData
• Year of publication: 2022
• Journal volume: 7
• Journal issue: 6
• Pages of publication: x220627
• a: 8.9701 ± 0.0003 Å
• b: 13.2202 ± 0.0005 Å
• c: 14.0861 ± 0.0005 Å
• α: 99.609 ± 0.003°
• β: 103.133 ± 0.003°
• γ: 107.676 ± 0.003°
• Cell volume: 1499 ± 0.1 ų
• Cell temperature: 263 ± 1 K
• Ambient diffraction temperature: 263 ± 1 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0685
• Residual factor for significantly intense reflections: 0.0402
• Weighted residual factors for significantly intense reflections: 0.0945
• Weighted residual factors for all reflections included in the refinement: 0.1012
• Goodness-of-fit parameter for all reflections included in the refinement: 0.828
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.56083 Å
• Diffraction radiation type: AgKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes