Crystallography Open Database

Information card for entry 1567522

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Coordinates	1567522.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34 H36 Cl P2 Rh
Calculated formula	C34 H36 Cl P2 Rh
Title of publication	Direct Method to Access Various Functional Arylalkoxysilanes by Rh-catalysed Intermolecular C–H Silylation of Alkoxysilane
Authors of publication	Som, Salina; Choi, Jongwook; Katsoulis, Dimitris; Lee, Kangsang L.
Journal of publication	Chemical Science
Year of publication	2022
a	10.3091 ± 0.0003 Å
b	12.7665 ± 0.0004 Å
c	13.3424 ± 0.0004 Å
α	107.864 ± 0.001°
β	101.093 ± 0.001°
γ	112.099 ± 0.001°
Cell volume	1451.17 ± 0.08 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	1
Hermann-Mauguin space group symbol	P 1
Hall space group symbol	P 1
Residual factor for all reflections	0.0227
Residual factor for significantly intense reflections	0.0203
Weighted residual factors for significantly intense reflections	0.0459
Weighted residual factors for all reflections included in the refinement	0.0469
Goodness-of-fit parameter for all reflections included in the refinement	1.03
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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