Information card for entry 1567595

Structure parameters

• Chemical name: HSnNi3(dppm)3H
• Formula: C79 H77 Ni3 O P6 Sn
• Calculated formula: C79 H77 Ni3 O P6 Sn
• Title of publication: Synthesis, Structure and Reactivity of µ3-SnH Capped Trinuclear Nickel Cluster
• Authors of publication: Torquato, Nicole A.; Mrse, Anthony A.; Gembicky, Milan; Chan, Thomas; Brunner, Felix M.; Kubiak, Clifford P.; Bertrand, Quentin C.; Palasz, Joseph M.
• Journal of publication: Chemical Science
• Year of publication: 2022
• a: 15.7957 ± 0.0016 Å
• b: 15.853 ± 0.0016 Å
• c: 15.9408 ± 0.0016 Å
• α: 88.234 ± 0.001°
• β: 74.099 ± 0.001°
• γ: 85.076 ± 0.001°
• Cell volume: 3824.7 ± 0.7 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0536
• Residual factor for significantly intense reflections: 0.0434
• Weighted residual factors for significantly intense reflections: 0.1084
• Weighted residual factors for all reflections included in the refinement: 0.1177
• Goodness-of-fit parameter for all reflections included in the refinement: 1.035
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Diffraction radiation X-ray symbol: K-L~3~
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No