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Information card for entry 1567608
Preview
Jmol._Canvas2D (Jmol) "jmolApplet0"[x]
Coordinates | 1567608.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C23 H29 N |
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Calculated formula | C23 H29 N |
Title of publication | Palladium/GF-Phos-catalyzed asymmetric carbenylative amination to access chiral pyrrolidines and piperidines |
Authors of publication | Sun, Yue; Ma, Chun; Li, Zhiming; Zhang, Junliang |
Journal of publication | Chemical Science |
Year of publication | 2022 |
Journal volume | 13 |
Journal issue | 37 |
Pages of publication | 11150 - 11155 |
a | 10.9102 ± 0.0003 Å |
b | 6.1038 ± 0.0002 Å |
c | 14.7452 ± 0.0004 Å |
α | 90° |
β | 99.5 ± 0.003° |
γ | 90° |
Cell volume | 968.47 ± 0.05 Å3 |
Cell temperature | 173 ± 0.1 K |
Ambient diffraction temperature | 173 ± 0.1 K |
Number of distinct elements | 3 |
Space group number | 4 |
Hermann-Mauguin space group symbol | P 1 21 1 |
Hall space group symbol | P 2yb |
Residual factor for all reflections | 0.0491 |
Residual factor for significantly intense reflections | 0.0465 |
Weighted residual factors for significantly intense reflections | 0.1281 |
Weighted residual factors for all reflections included in the refinement | 0.1301 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.039 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/1567608.html
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structural data.