Information card for entry 1567632
| Formula |
C25 H30 N2 O2 |
| Calculated formula |
C25 H30 N2 O2 |
| Title of publication |
Palladium-catalyzed intramolecular Heck dearomative <i>gem</i>-difluorovinylation of indoles. |
| Authors of publication |
Wang, Gang; Li, Wenqi; Liu, Tianxiang; Zhang, Yonghong; Wang, Bin; Xue, Fei; Jin, Weiwei; Ma, Caiyan; Xia, Yu; Liu, Chenjiang |
| Journal of publication |
Chemical science |
| Year of publication |
2022 |
| Journal volume |
13 |
| Journal issue |
39 |
| Pages of publication |
11594 - 11599 |
| a |
20.192 ± 0.0008 Å |
| b |
20.192 ± 0.0008 Å |
| c |
11.043 ± 0.0005 Å |
| α |
90° |
| β |
90° |
| γ |
90° |
| Cell volume |
4502.4 ± 0.3 Å3 |
| Cell temperature |
296.15 K |
| Ambient diffraction temperature |
296.15 K |
| Number of distinct elements |
4 |
| Space group number |
114 |
| Hermann-Mauguin space group symbol |
P -4 21 c |
| Hall space group symbol |
P -4 2n |
| Residual factor for all reflections |
0.1518 |
| Residual factor for significantly intense reflections |
0.0709 |
| Weighted residual factors for significantly intense reflections |
0.1481 |
| Weighted residual factors for all reflections included in the refinement |
0.1737 |
| Goodness-of-fit parameter for all reflections included in the refinement |
0.952 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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The link is:
https://www.crystallography.net/1567632.html
