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Information card for entry 1567781
Preview
Coordinates | 1567781.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C11 H14 F Fe O2 P |
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Calculated formula | C11 H13.928 F Fe O2 P |
Title of publication | Synthesis of phosphiranes <i>via</i> organoiron-catalyzed phosphinidene transfer to electron-deficient olefins. |
Authors of publication | Xin, Tiansi; Geeson, Michael B.; Zhu, Hui; Qu, Zheng-Wang; Grimme, Stefan; Cummins, Christopher C. |
Journal of publication | Chemical science |
Year of publication | 2022 |
Journal volume | 13 |
Journal issue | 43 |
Pages of publication | 12696 - 12702 |
a | 21.4541 ± 0.0005 Å |
b | 9.6814 ± 0.0002 Å |
c | 23.524 ± 0.0005 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 4886.07 ± 0.18 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 6 |
Space group number | 61 |
Hermann-Mauguin space group symbol | P b c a |
Hall space group symbol | -P 2ac 2ab |
Residual factor for all reflections | 0.0428 |
Residual factor for significantly intense reflections | 0.0323 |
Weighted residual factors for significantly intense reflections | 0.081 |
Weighted residual factors for all reflections included in the refinement | 0.0877 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.039 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/1567781.html
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