Information card for entry 1568014

Structure parameters

• Formula: C32 H36 Cl3 P2 Re
• Calculated formula: C32 H36 Cl3 P2 Re
• Title of publication: Synthesis and characterization of bi(metallacycloprop-1-ene) complexes.
• Authors of publication: Bai, Wei; Tsang, Long Yiu; Wang, Yilun; Li, Yang; Sung, Herman H. Y.; Williams, Ian D.; Jia, Guochen
• Journal of publication: Chemical science
• Year of publication: 2022
• Journal volume: 14
• Journal issue: 1
• Pages of publication: 96 - 102
• a: 11.082 ± 0.0002 Å
• b: 18.4374 ± 0.0003 Å
• c: 15.6667 ± 0.0003 Å
• α: 90°
• β: 107.276 ± 0.002°
• γ: 90°
• Cell volume: 3056.66 ± 0.1 ų
• Cell temperature: 100.01 ± 0.1 K
• Ambient diffraction temperature: 100.15 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0174
• Residual factor for significantly intense reflections: 0.0167
• Weighted residual factors for significantly intense reflections: 0.0417
• Weighted residual factors for all reflections included in the refinement: 0.0421
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No