Information card for entry 1568385
| Formula |
C24 H21 F N2 O4 |
| Calculated formula |
C24 H21 F N2 O4 |
| Title of publication |
Intramolecular trapping of spiro radicals to produce unusual cyclization products from usual migration substrates |
| Authors of publication |
Zhang, Jingming; Liu, Chengkou; Qiao, Yaqi; Wei, Minghui; Guan, Wenjing; Mao, Ziren; Qin, Hong; Fang, Zheng; Guo, Kai |
| Journal of publication |
Chemical Science |
| Year of publication |
2023 |
| Journal volume |
14 |
| Journal issue |
9 |
| Pages of publication |
2461 - 2466 |
| a |
8.8055 ± 0.0007 Å |
| b |
11.8006 ± 0.0009 Å |
| c |
19.3349 ± 0.0015 Å |
| α |
90° |
| β |
91.749 ± 0.004° |
| γ |
90° |
| Cell volume |
2008.2 ± 0.3 Å3 |
| Cell temperature |
193 K |
| Ambient diffraction temperature |
193 K |
| Number of distinct elements |
5 |
| Space group number |
14 |
| Hermann-Mauguin space group symbol |
P 1 21/n 1 |
| Hall space group symbol |
-P 2yn |
| Residual factor for all reflections |
0.0676 |
| Residual factor for significantly intense reflections |
0.049 |
| Weighted residual factors for significantly intense reflections |
0.1247 |
| Weighted residual factors for all reflections included in the refinement |
0.1382 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.057 |
| Diffraction radiation wavelength |
1.34139 Å |
| Diffraction radiation type |
GaKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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The link is:
https://www.crystallography.net/1568385.html
