Information card for entry 1568452

Structure parameters

• Formula: C35 H34 N2 O
• Calculated formula: C35 H34 N2 O
• Title of publication: Metal-free photosensitized radical relay 1,4-carboimination across two distinct olefins
• Authors of publication: Tan, Guangying; Paulus, Fritz; Petti, Alessia; Wiethoff, Maxim-Aleksa; Lauer, Anna; Daniliuc, Constantin; Glorius, Frank
• Journal of publication: Chemical Science
• Year of publication: 2023
• Journal volume: 14
• Journal issue: 9
• Pages of publication: 2447 - 2454
• a: 9.3198 ± 0.0003 Å
• b: 11.1833 ± 0.0004 Å
• c: 26.6506 ± 0.0007 Å
• α: 90°
• β: 99.812 ± 0.001°
• γ: 90°
• Cell volume: 2737.06 ± 0.15 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.057
• Residual factor for significantly intense reflections: 0.0423
• Weighted residual factors for significantly intense reflections: 0.0926
• Weighted residual factors for all reflections included in the refinement: 0.1006
• Goodness-of-fit parameter for all reflections included in the refinement: 1.059
• Diffraction radiation probe: single crystal
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No