Information card for entry 1568649

Structure parameters

• Formula: C55 H65 Cl N2 O P3 Rh
• Calculated formula: C55 H65 Cl N2 O P3 Rh
• Title of publication: Probing the donor strength of yldiide ligands: synthesis, structure and reactivity of rhodium complexes with a PC_ylideN pincer ligand.
• Authors of publication: Lapointe, Sébastien; Duari, Prakash; Gessner, Viktoria H.
• Journal of publication: Chemical science
• Year of publication: 2023
• Journal volume: 14
• Journal issue: 14
• Pages of publication: 3816 - 3825
• a: 11.6926 ± 0.0001 Å
• b: 14.4062 ± 0.0002 Å
• c: 16.2053 ± 0.0002 Å
• α: 105.002 ± 0.001°
• β: 95.705 ± 0.001°
• γ: 98.036 ± 0.001°
• Cell volume: 2584.42 ± 0.06 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0421
• Residual factor for significantly intense reflections: 0.0319
• Weighted residual factors for significantly intense reflections: 0.0798
• Weighted residual factors for all reflections included in the refinement: 0.0844
• Goodness-of-fit parameter for all reflections included in the refinement: 1.035
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No