Information card for entry 1568728

Structure parameters

• Formula: C46 H58 B Cl Si
• Calculated formula: C46.003 H58.009 B Cl Si
• Title of publication: Catalyst-free diboration and silaboration of alkenes and alkynes using bis(9-heterofluorenyl)s.
• Authors of publication: Gilmer, Jannik; Trageser, Timo; Čaić, Luis; Virovets, Alexander; Bolte, Michael; Lerner, Hans-Wolfram; Fantuzzi, Felipe; Wagner, Matthias
• Journal of publication: Chemical science
• Year of publication: 2023
• Journal volume: 14
• Journal issue: 17
• Pages of publication: 4589 - 4596
• a: 9.8879 ± 0.0012 Å
• b: 14.446 ± 0.002 Å
• c: 16.292 ± 0.003 Å
• α: 115.332 ± 0.015°
• β: 91.157 ± 0.011°
• γ: 102.693 ± 0.011°
• Cell volume: 2034.7 ± 0.6 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1227
• Residual factor for significantly intense reflections: 0.0705
• Weighted residual factors for significantly intense reflections: 0.1721
• Weighted residual factors for all reflections included in the refinement: 0.2006
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No