Information card for entry 1568732

Structure parameters

• Formula: C46 H60 B Cl Si
• Calculated formula: C46 H60 B Cl Si
• Title of publication: Catalyst-free diboration and silaboration of alkenes and alkynes using bis(9-heterofluorenyl)s.
• Authors of publication: Gilmer, Jannik; Trageser, Timo; Čaić, Luis; Virovets, Alexander; Bolte, Michael; Lerner, Hans-Wolfram; Fantuzzi, Felipe; Wagner, Matthias
• Journal of publication: Chemical science
• Year of publication: 2023
• Journal volume: 14
• Journal issue: 17
• Pages of publication: 4589 - 4596
• a: 11.9435 ± 0.0008 Å
• b: 24.517 ± 0.002 Å
• c: 15.0825 ± 0.0012 Å
• α: 90°
• β: 103.854 ± 0.008°
• γ: 90°
• Cell volume: 4288 ± 0.6 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1199
• Residual factor for significantly intense reflections: 0.0582
• Weighted residual factors for significantly intense reflections: 0.1051
• Weighted residual factors for all reflections included in the refinement: 0.1271
• Goodness-of-fit parameter for all reflections included in the refinement: 0.956
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No