Information card for entry 1568735

Structure parameters

• Formula: C55 H69 B Cl Si
• Calculated formula: C55 H69 B Cl Si
• Title of publication: Catalyst-free diboration and silaboration of alkenes and alkynes using bis(9-heterofluorenyl)s.
• Authors of publication: Gilmer, Jannik; Trageser, Timo; Čaić, Luis; Virovets, Alexander; Bolte, Michael; Lerner, Hans-Wolfram; Fantuzzi, Felipe; Wagner, Matthias
• Journal of publication: Chemical science
• Year of publication: 2023
• Journal volume: 14
• Journal issue: 17
• Pages of publication: 4589 - 4596
• a: 9.8384 ± 0.0007 Å
• b: 14.6699 ± 0.0011 Å
• c: 17.434 ± 0.0013 Å
• α: 92.485 ± 0.006°
• β: 98.376 ± 0.006°
• γ: 102.215 ± 0.006°
• Cell volume: 2425.9 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1526
• Residual factor for significantly intense reflections: 0.0749
• Weighted residual factors for significantly intense reflections: 0.1536
• Weighted residual factors for all reflections included in the refinement: 0.189
• Goodness-of-fit parameter for all reflections included in the refinement: 1.014
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No