Information card for entry 1569011

Structure parameters

• Formula: C59 H86 Ge K N3 O3
• Calculated formula: C59 H86 Ge K N3 O3
• Title of publication: A crystalline T-shaped planar group 14 anion.
• Authors of publication: Liu, Xiaona; Dai, Yuyang; Bao, Manling; Wang, Wenjuan; Li, Qianli; Liu, Chunmeng; Wang, Xinping; Su, Yuanting
• Journal of publication: Chemical science
• Year of publication: 2023
• Journal volume: 14
• Journal issue: 21
• Pages of publication: 5722 - 5727
• a: 11.0177 ± 0.0007 Å
• b: 21.7711 ± 0.0013 Å
• c: 24.2953 ± 0.0016 Å
• α: 90°
• β: 92.991 ± 0.003°
• γ: 90°
• Cell volume: 5819.7 ± 0.6 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0589
• Residual factor for significantly intense reflections: 0.0492
• Weighted residual factors for significantly intense reflections: 0.1344
• Weighted residual factors for all reflections included in the refinement: 0.1407
• Goodness-of-fit parameter for all reflections included in the refinement: 1.0263
• Diffraction radiation wavelength: 1.34139 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No