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Information card for entry 1569112
Preview
Coordinates | 1569112.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C52 H54 N2 O15 |
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Calculated formula | C52 H54 N2 O15 |
Title of publication | Catalytic generation of <i>ortho</i>-quinone dimethides <i>via</i> donor/donor rhodium carbenes. |
Authors of publication | Gao, Mingchun; Ruiz, Jose M.; Jimenez, Emily; Lo, Anna; Laconsay, Croix J.; Fettinger, James C.; Tantillo, Dean J.; Shaw, Jared T. |
Journal of publication | Chemical science |
Year of publication | 2023 |
Journal volume | 14 |
Journal issue | 23 |
Pages of publication | 6443 - 6448 |
a | 9.7429 ± 0.0007 Å |
b | 14.3116 ± 0.001 Å |
c | 18.0645 ± 0.0012 Å |
α | 67.127 ± 0.0015° |
β | 81.542 ± 0.0016° |
γ | 80.5606 ± 0.0017° |
Cell volume | 2279.7 ± 0.3 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0554 |
Residual factor for significantly intense reflections | 0.0483 |
Weighted residual factors for significantly intense reflections | 0.1297 |
Weighted residual factors for all reflections included in the refinement | 0.1365 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.037 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/1569112.html
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Users of the data should acknowledge the original authors of the
structural data.