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Information card for entry 1569274
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Coordinates | 1569274.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C28 H27 N O2 S |
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Calculated formula | C28 H27 N O2 S |
Title of publication | An interrupted Corey-Chaykovsky reaction of designed azaarenium salts: synthesis of complex polycyclic spiro- and fused cyclopropanoids. |
Authors of publication | Singh, Bara; Ansari, Arshad J.; Malik, Nirmal; Ramasastry, S. S. V. |
Journal of publication | Chemical science |
Year of publication | 2023 |
Journal volume | 14 |
Journal issue | 25 |
Pages of publication | 6963 - 6969 |
a | 9.0157 ± 0.0003 Å |
b | 11.1293 ± 0.0004 Å |
c | 11.8264 ± 0.0003 Å |
α | 88.918 ± 0.003° |
β | 87.476 ± 0.003° |
γ | 74.544 ± 0.003° |
Cell volume | 1142.59 ± 0.07 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0743 |
Residual factor for significantly intense reflections | 0.0502 |
Weighted residual factors for significantly intense reflections | 0.1363 |
Weighted residual factors for all reflections included in the refinement | 0.149 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.12 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/1569274.html
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Users of the data should acknowledge the original authors of the
structural data.