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Information card for entry 1569346
Preview
Coordinates | 1569346.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C23 H25 N O3 S |
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Calculated formula | C23 H25 N O3 S |
Title of publication | Palladium-catalyzed intramolecular asymmetric hydrocyclopropanylation of alkynes: synthesis of cyclopropane-fused γ-lactams. |
Authors of publication | Lin, Han-Ze; Qi, Zhuang; Wu, Qi-Min; Jiang, Yong-Yu; Peng, Jin-Bao |
Journal of publication | Chemical science |
Year of publication | 2023 |
Journal volume | 14 |
Journal issue | 27 |
Pages of publication | 7564 - 7568 |
a | 15.4147 ± 0.0005 Å |
b | 10.4118 ± 0.0004 Å |
c | 12.7924 ± 0.0004 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 2053.11 ± 0.12 Å3 |
Cell temperature | 298.37 ± 0.1 K |
Ambient diffraction temperature | 298.37 ± 0.1 K |
Number of distinct elements | 5 |
Space group number | 33 |
Hermann-Mauguin space group symbol | P n a 21 |
Hall space group symbol | P 2c -2n |
Residual factor for all reflections | 0.0592 |
Residual factor for significantly intense reflections | 0.0548 |
Weighted residual factors for significantly intense reflections | 0.1463 |
Weighted residual factors for all reflections included in the refinement | 0.153 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.015 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/1569346.html
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