Crystallography Open Database

Information card for entry 1569576

Preview

Coordinates	1569576.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C102 H90 Na2 O2 P6 Rh2
Calculated formula	C102 H90 Na2 O2 P6 Rh2
Title of publication	A dinuclear Rh(-i)/Rh(i) complex bridged by biphilic phosphinine ligands.
Authors of publication	Masada, Koichiro; Okabe, Kiyosumi; Kusumoto, Shuhei; Nozaki, Kyoko
Journal of publication	Chemical science
Year of publication	2023
Journal volume	14
Journal issue	32
Pages of publication	8524 - 8530
a	13.1385 ± 0.0002 Å
b	16.5943 ± 0.0002 Å
c	20.896 ± 0.0003 Å
α	93.698 ± 0.001°
β	91.535 ± 0.001°
γ	98.479 ± 0.001°
Cell volume	4493.61 ± 0.11 Å³
Cell temperature	93 ± 2 K
Ambient diffraction temperature	93.15 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0916
Residual factor for significantly intense reflections	0.0739
Weighted residual factors for significantly intense reflections	0.1955
Weighted residual factors for all reflections included in the refinement	0.2075
Goodness-of-fit parameter for all reflections included in the refinement	1.03
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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