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Information card for entry 1569880
Preview
Coordinates | 1569880.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C27 H22 N2 O2 |
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Calculated formula | C27 H22 N2 O2 |
Title of publication | Rh(iii)-catalyzed highly site- and regio-selective alkenyl C-H activation/annulation of 4-amino-2-quinolones with alkynes <i>via</i> reversible alkyne insertion. |
Authors of publication | Hirako, Naohiro; Yasui, Takeshi; Yamamoto, Yoshihiko |
Journal of publication | Chemical science |
Year of publication | 2023 |
Journal volume | 14 |
Journal issue | 39 |
Pages of publication | 10971 - 10978 |
a | 9.0396 ± 0.0015 Å |
b | 21.882 ± 0.004 Å |
c | 10.4133 ± 0.0018 Å |
α | 90° |
β | 97.221 ± 0.004° |
γ | 90° |
Cell volume | 2043.5 ± 0.6 Å3 |
Cell temperature | 273 K |
Ambient diffraction temperature | 273 K |
Number of distinct elements | 4 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0706 |
Residual factor for significantly intense reflections | 0.0524 |
Weighted residual factors for significantly intense reflections | 0.1122 |
Weighted residual factors for all reflections included in the refinement | 0.1152 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.824 |
Diffraction radiation wavelength | 0.71075 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/1569880.html
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