Information card for entry 1570288

Structure parameters

• Formula: C68 H40 Cl F40 N Sb4
• Calculated formula: C68 H40 Cl F40 N Sb4
• Title of publication: Poly-pnictogen bonding: trapping halide ions by a tetradentate antimony(iii) Lewis acid.
• Authors of publication: Beckmann, J. Louis; Krieft, Jonas; Vishnevskiy, Yury V.; Neumann, Beate; Stammler, Hans-Georg; Mitzel, Norbert W.
• Journal of publication: Chemical science
• Year of publication: 2023
• Journal volume: 14
• Journal issue: 46
• Pages of publication: 13551 - 13559
• a: 15.7731 ± 0.0002 Å
• b: 21.2235 ± 0.0004 Å
• c: 22.9543 ± 0.0004 Å
• α: 90°
• β: 102.695 ± 0.002°
• γ: 90°
• Cell volume: 7496.3 ± 0.2 ų
• Cell temperature: 100 ± 0.1 K
• Ambient diffraction temperature: 100 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0988
• Residual factor for significantly intense reflections: 0.0885
• Weighted residual factors for significantly intense reflections: 0.2426
• Weighted residual factors for all reflections included in the refinement: 0.253
• Goodness-of-fit parameter for all reflections included in the refinement: 1.058
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No