Information card for entry 1570320

Structure parameters

• Formula: C66 H60 Cl4 F6 Ge N4 O6 P2 S2
• Calculated formula: C66 H60 Cl4 F6 Ge N4 O6 P2 S2
• Title of publication: Intramolecular donor-stabilized tetra-coordinated germanium(iv) di-cations and their Lewis acidic properties.
• Authors of publication: Peddi, Balakrishna; Khan, Souvik; Gonnade, Rajesh G.; Yildiz, Cem B.; Majumdar, Moumita
• Journal of publication: Chemical science
• Year of publication: 2023
• Journal volume: 14
• Journal issue: 47
• Pages of publication: 13755 - 13764
• a: 13.652 ± 0.003 Å
• b: 15.573 ± 0.003 Å
• c: 16.333 ± 0.003 Å
• α: 79.755 ± 0.006°
• β: 79.751 ± 0.006°
• γ: 71.778 ± 0.006°
• Cell volume: 3217.8 ± 1.1 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 9
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.129
• Residual factor for significantly intense reflections: 0.0722
• Weighted residual factors for significantly intense reflections: 0.1826
• Weighted residual factors for all reflections included in the refinement: 0.2102
• Goodness-of-fit parameter for all reflections included in the refinement: 1.053
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No