Information card for entry 1570326

Structure parameters

• Formula: C55 H49 F3 Ge O4 P2 S
• Calculated formula: C55 H49 F3 Ge O4 P2 S
• Title of publication: Intramolecular donor-stabilized tetra-coordinated germanium(iv) di-cations and their Lewis acidic properties.
• Authors of publication: Peddi, Balakrishna; Khan, Souvik; Gonnade, Rajesh G.; Yildiz, Cem B.; Majumdar, Moumita
• Journal of publication: Chemical science
• Year of publication: 2023
• Journal volume: 14
• Journal issue: 47
• Pages of publication: 13755 - 13764
• a: 12.192 ± 0.002 Å
• b: 21.924 ± 0.004 Å
• c: 18.159 ± 0.004 Å
• α: 90 ± 0.03°
• β: 103.59 ± 0.03°
• γ: 90 ± 0.03°
• Cell volume: 4718 ± 1.7 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.048
• Residual factor for significantly intense reflections: 0.0383
• Weighted residual factors for significantly intense reflections: 0.0938
• Weighted residual factors for all reflections included in the refinement: 0.1006
• Goodness-of-fit parameter for all reflections included in the refinement: 1.054
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No