Crystallography Open Database

Information card for entry 1570345

Preview

Coordinates	1570345.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	fluoro(mesityl)(2,3,4,5,6-pentamethylphenyl)borane
Formula	C20 H26 B F
Calculated formula	C20 H26 B F
Title of publication	Rapid, iterative syntheses of unsymmetrical di- and triarylboranes from crystalline aryldifluoroboranes.
Authors of publication	Turnbull, Douglas; Légaré, Marc-André
Journal of publication	Chemical science
Year of publication	2023
Journal volume	14
Journal issue	48
Pages of publication	14256 - 14261
a	8.6399 ± 0.0004 Å
b	25.3455 ± 0.0011 Å
c	8.6121 ± 0.0003 Å
α	90°
β	114.716 ± 0.002°
γ	90°
Cell volume	1713.14 ± 0.13 Å³
Cell temperature	273 ± 2 K
Ambient diffraction temperature	150 K
Number of distinct elements	4
Space group number	9
Hermann-Mauguin space group symbol	C 1 c 1
Hall space group symbol	C -2yc
Residual factor for all reflections	0.0458
Residual factor for significantly intense reflections	0.041
Weighted residual factors for significantly intense reflections	0.106
Weighted residual factors for all reflections included in the refinement	0.1093
Goodness-of-fit parameter for all reflections included in the refinement	1.0411
Diffraction radiation wavelength	1.34139 Å
Diffraction radiation type	synchrotron
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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